HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → 3-Methylpyridine-2-carboxaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 178426302 | HCID 178426302 | — |
| Product | 3-Methylpyridine-2-carboxaldehyde | HCID 1501874 | 33% |
Reaction Steps
3-Methyl-pyridine-2-carbaldehyde (200 mg, 33.0%) was obtained from 0.25 M 3-methyl-2-pyridinylmagnesium bromide of THF solution (20 mL, 5 mmol) with DMF (0.773 mL, 10 mmol) at room temperature under argon.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07074809B2 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-fafd068689ee495580217a21665ecd92 |
| Source note | uspto-grants-2006_07 |