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3-(Trifluoromethyl)benzoyl chloride → N'-(2-phenoxypyridine-3-carbonyl)-3-(trifluoromethyl)benzhydrazide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-(Trifluoromethyl)benzoyl chloride | HCID 75257 | — |
| 反応物 | 2-Phenoxynicotinohydrazide | HCID 2797685 | — |
| 溶媒 | Pyridine | HCID 1049 | — |
| 生成物 | N'-(2-phenoxypyridine-3-carbonyl)-3-(trifluoromethyl)benzhydrazide | HCID 2797700 | — |
反応手順
Alternatively, as shown in scheme 2, reaction of 2-phenoxy-nicotinic acid hydrazide with 3-trifluoromethyl-benzoyl chloride in the presence of a base such as pyridine produced N′-(2-phenoxypyridine-3-carbonyl)-3-(trifluoromethyl)benzhydrazide as the product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07074813B2 |
| 出典データセット | uspto-grants-2006_07 |
| ORD ID | ord-36064edae2b34b68bc893389bcce80b2 |
| 出典メモ | uspto-grants-2006_07 |