HCID 131725852, compound → HCID 22033936, compound

Participants

Reaction Steps

The title compound was prepared in the same manner as Example 3B) from lithium (1-ethyl-2-phenyl-1,2-azaborolide) (1C), 0.41 g, 2.31 mmol) in 15 mL of THF and 1-ethyl-3-chlorodimethylsilyl-2,3-dihydro-2-phenyl-1H-1,2-azaborole (Ex. 3A), 0.01 g, 2.31 mmol) in 15 mL of THF. The product was obtained as a yellow oil (0.85 g, 92 percent).

Provenance & Evidence