HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 22030969, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Bromobutyronitrile | HCID 21412 | — |
| Reactant | 2-Thiophenethiol | HCID 522674 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 22030969 | HCID 22030969 | 93.7% |
Reaction Steps
2.3 g of thiophen-2-thiol, 3.0 g of 4-bromobutyronitrile and 5.5 g of potassium carbonate were stirred in N,N-dimethylformamide at room temperature to give 3.4 g of 4-(2-thienylsulfanyl)butane nitrile. 3.4 g of 4-(2-thienylsulfanyl)butane nitrile was reacted with 5.4 g of N-iodosuccinimide in N,N-dimethylformamide, whereby 5.5 g of the title compound was obtained as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07074801B1 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-ea58fd028a1c48f494e56cfad00eee8d |
| Source note | uspto-grants-2006_07 |