HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Ethenylpyridin-2-amine → 5-Ethylpyridin-2-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Ethenylpyridin-2-amine | HCID 22032080 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 5-Ethylpyridin-2-amine | HCID 9812777 | 94.4% |
Reaction Steps
0.25 g 5-vinylpyridin-2-yl amine (compound in Production Example 326) and 0.1 g of 10% palladium-carbon were stirred in 5 mL ethyl acetate at room temperature for 2 hours under hydrogen atmosphere. The reaction solution was purified by NH silica gel column chromatography (ethyl acetate), to give 0.24 g of the title compound as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07074801B1 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-09aab869bb414c14b748af51fb8fca97 |
| Source note | uspto-grants-2006_07 |