HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22032084, compound → HCID 23537722, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22032084 | HCID 22032084 | — |
| Reactant | HCID 23537547 | HCID 23537547 | — |
| Product | HCID 23537722 | HCID 23537722 | 29.5% |
Reaction Steps
131 mg 5-(6-bromoquinazolin-4-yl)-thiophen-2-sulfonic acid (2-dimethylaminoethyl)-methyl-amide (compound in Production Example 376) and 168 mg 3-(4-fluorophenyl)-1-trityl-1H-4-pyrazolylboronic acid (compound in Production Example 25) were subjected to the same reaction as in Example 9, and the isomer was separated and purified by a column to give 66 mg of the title compound as yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07074801B1 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-da0dc740f31e4605bb435722d797ebf9 |
| Source note | uspto-grants-2006_07 |