Hydroxylamine, O-ethyl- → 4-{N-(6-Chloro-3-pyridazinyl)-N-methyl-5-aminopentan-1-oxy}benzaldehyde O-ethyloxime
반응식
[Cl:1][C:2]1[N:7]=[N:6][C:5]([N:8]([CH3:23])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][O:14][C:15]2[CH:22]=[CH:21][C:18]([CH:19]=O)=[CH:17][CH:16]=2)=[CH:4][CH:3]=1.[CH2:24]([O:26][NH2:27])[CH3:25]>>[CH2:24]([O:26][N:27]=[CH:19][C:18]1[CH:21]=[CH:22][C:15]([O:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][N:8]([C:5]2[N:6]=[N:7][C:2]([Cl:1])=[CH:3][CH:4]=2)[CH3:23])=[CH:16][CH:17]=1)[CH3:25]참가 물질
3
실험 절차
Reaction of 4-{N-(6-Chloro-3-pyridazinyl)-N-methyl-5-aminopentan-1-oxy}benzaldehyde with ethoxyamine following similar conditions to those in Example 1 gave 4-{N-(6-Chloro-3-pyridazinyl)-N-methyl-5-aminopentan-1-oxy}benzaldehyde O-ethyloxime (Compound 161) as a colourless oil. The nmr and mass spectral data are given below in Table 11.
출처 및 근거
- ORD 기록
- ord-6c0677b2b364456290183131bbb7d1a5
- 출처 데이터셋
- uspto-grants-2006_07
- 특허 번호
- US07078403B1
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