Carbon Dioxide → HCID 178506955, compound

Participants

Reaction Steps

FSO2(CF2)4OCH3 (35.8 g, 0.114 mole) was treated with lithium hydroxide monohydrate (12 g, 0.285 mole) in deionized water (150 g) at 75° C. for six hours. After cooling to room temperature, two small pieces of solid carbon dioxide (Dry Ice) were added to neutralize the excess lithium hydroxide. The water was removed by using a rotary evaporator and the residue extracted with alcohol as described in Preparation of Precursor 1 above to yield LiO3S(CF2)4OCH3.

Provenance & Evidence