HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopentylamine → 1-cyclopentyl-4-nitro-1H-imidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopentylamine | HCID 2906 | — |
| Reactant | 1,4-Dinitro-1H-imidazole | HCID 5169496 | — |
| Product | 1-cyclopentyl-4-nitro-1H-imidazole | HCID 22025989 | 75% |
Reaction Steps
This reaction was carried out using the procedure for Preparation 1 with cyclopentyl amine and 1,4-dinitroimidazole to afford 205 mg (75% yield) of 1-cyclopentyl-4-nitro-1H-imidazole; 1H NMR (400 MHz, CDCl3) δ 7.77 (s, 1H), 7.45 (s, 1H), 4.49 (m, 1H), 2.25 (m, 2H), 2.0–1.7 (m, 6H); MS (AP/CI): 182.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07078529B2 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-394e4d26bd894add8e909419ab362dae |
| Source note | uspto-grants-2006_07 |