Azobisisobutyronitrile → HCID 86595653, compound

Participants

Reaction Steps

To tetrahydrofuran (250 g) and methylethylketone (250 g) were added methylmethacrylate (40 g), 2-hydroxyethylmethacrylate (30 g), acrylic acid (30 g) and AIBN (2.5 g). The resulting mixture was reacted at 66° C. for 8 hours. After reaction, the resulting mixture was precipitated in ether, filtered, and dehydrated, thereby obtaining poly(methylmethacrylate/2-hydroxyethylmethacrylate/acrylic acid) (86 g). The polystyrene converted number average molecular weight of poly(methylmethacrylate/2-hydroxyethyl methacrylate/acrylic acid) was 17,500.

Provenance & Evidence