HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromoacetate → HCID 10363179, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | (4-Methoxyphenyl)-(3-(naphthalen-2-yloxy)propyl)amine | HCID 9839556 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 10363179 | HCID 10363179 | — |
Reaction Steps
A mixture of (4-methoxyphenyl)-(3-(naphthalen-2-yloxy)propyl)amine (0.5 gm, 0.002 mole) and ethyl bromoacetate (0.62 ml, 0.003 mole) was taken in dry acetone (40 ml). It was refluxed for 10 hrs and the progress of reaction checked by TLC. Reaction mixture was filtered and the filtrate was concentrated to get the oily compound {N-(4-methoxy phenyl)-(3-(naphthalen-2-yloxy)propyl)amino}acetic acid ethyl ester, oil (yield 0.75 ml, 96%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07081465B2 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-de5caab12b234d198645976888681713 |
| Source note | uspto-grants-2006_07 |