2,4-Dichlorobenzylidenemalononitrile → HCID 10309166, compound

HRID 1793897Notes

Reaction equation

HRID 1793897 reaction equation
[N:1]1([C:8]([NH2:10])=[NH:9])[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[Cl:11][C:12]1[CH:23]=[C:22]([Cl:24])[CH:21]=[CH:20][C:13]=1[CH:14]=[C:15]([C:18]#[N:19])[C:16]#[N:17]>>[NH2:19][CH2:18][C:15]1[C:16]([NH2:17])=[N:9][C:8]([N:1]2[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]2)=[N:10][C:14]=1[C:13]1[CH:20]=[CH:21][C:22]([Cl:24])=[CH:23][C:12]=1[Cl:11]

Participants

3

Reactant 2

HCID 180892,4-DichlorobenzylidenemalononitrileHCID 13237004HCID 13237004, compound

Product 1

HCID 10309166HCID 10309166, compound

Procedure

The title compound, MS: m/e=366.0 (M+H+), was prepared from azepane-1-carboxamidine and 2-(2,4-dichloro-benzylidene)-malononitrile in analogy to the process described in Example 11 as a solid.

Sources & evidence

ORD record
ord-fd10456043014940a3721c0ac9868bc8
Source dataset
uspto-grants-2006_04
Patent number
US07022718B2

Reaction notes

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