2-Methyl-2-thiopseudourea → HCID 10286443, compound
Reaction equation
[CH3:1][S:2][C:3](=[NH:5])[NH2:4].[Cl:6][C:7]1[CH:18]=[C:17]([Cl:19])[CH:16]=[CH:15][C:8]=1[CH:9]=[C:10]([C:13]#[N:14])[C:11]#[N:12]>>[NH2:14][CH2:13][C:10]1[C:11]([NH2:12])=[N:5][C:3]([S:2][CH3:1])=[N:4][C:9]=1[C:8]1[CH:15]=[CH:16][C:17]([Cl:19])=[CH:18][C:7]=1[Cl:6]Participants
3
Procedure
The title compound, MS: m/e=315.2 (M+), was prepared from 2-methyl-isothiourea and 2-(2,4-dichloro-benzylidene)-malononitrile in analogy to the process described in Example 11 as a solid.
Sources & evidence
- ORD record
- ord-7a1418b735f1445ea9d093c6da418e34
- Source dataset
- uspto-grants-2006_04
- Patent number
- US07022718B2
Reaction notes
Loading…