2,4-Dichlorobenzylidenemalononitrile → HCID 10287361, compound

HRID 1793909Notes

Reaction equation

HRID 1793909 reaction equation
[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([C:10]([NH2:12])=[NH:11])=[CH:9][C:4]=2[O:3][CH2:2]1.[Cl:13][C:14]1[CH:25]=[C:24]([Cl:26])[CH:23]=[CH:22][C:15]=1[CH:16]=[C:17]([C:20]#[N:21])[C:18]#[N:19]>>[NH2:21][CH2:20][C:17]1[C:18]([NH2:19])=[N:11][C:10]([C:8]2[CH:7]=[CH:6][C:5]3[O:1][CH2:2][O:3][C:4]=3[CH:9]=2)=[N:12][C:16]=1[C:15]1[CH:22]=[CH:23][C:24]([Cl:26])=[CH:25][C:14]=1[Cl:13]

Participants

3

Reactant 2

HCID 180892,4-DichlorobenzylidenemalononitrileHCID 3654230HCID 3654230, compound

Product 1

HCID 10287361HCID 10287361, compound

Procedure

The title compound, MS: m/e=388.2 (M+), was prepared from benzo[1,3]dioxole-5-carboxamidine and 2-(2,4-dichloro-benzylidene)-malononitrile in analogy to the process described in Example 11 as a solid.

Sources & evidence

ORD record
ord-1b9949cae99d48d09ccc890d75c797e2
Source dataset
uspto-grants-2006_04
Patent number
US07022718B2

Reaction notes

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