2,4-Dichlorobenzylidenemalononitrile → HCID 10173174, compound

HRID 1793910Notes

Reaction equation

HRID 1793910 reaction equation
[F:1][C:2]([F:13])([F:12])[C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][CH:11]=1)[C:6]([NH2:8])=[NH:7].[Cl:14][C:15]1[CH:26]=[C:25]([Cl:27])[CH:24]=[CH:23][C:16]=1[CH:17]=[C:18]([C:21]#[N:22])[C:19]#[N:20]>>[NH2:22][CH2:21][C:18]1[C:19]([NH2:20])=[N:7][C:6]([C:5]2[CH:9]=[CH:10][CH:11]=[C:3]([C:2]([F:12])([F:13])[F:1])[CH:4]=2)=[N:8][C:17]=1[C:16]1[CH:23]=[CH:24][C:25]([Cl:27])=[CH:26][C:15]=1[Cl:14]

Participants

3

Reactant 2

HCID 180892,4-DichlorobenzylidenemalononitrileHCID 324537HCID 324537, compound

Product 1

HCID 10173174HCID 10173174, compound

Procedure

The title compound, MS: m/e=412.9 (M+H+), was prepared from 3-trifluoromethyl-benzamidine and 2-(2,4-dichloro-benzylidene)-malononitrile in analogy to the process described in Example 11 as a solid.

Sources & evidence

ORD record
ord-5164d2c9e42a45b08e7f639072d8348e
Source dataset
uspto-grants-2006_04
Patent number
US07022718B2

Reaction notes

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