HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiazole → HCID 22220633, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiazole | HCID 9256 | — |
| Reactant | Methyl bromoacetate | HCID 60984 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22220633 | HCID 22220633 | 66.8% |
Reaction Steps
Thiazole, (850 mg, 10 mmol), methyl bromoacetate (1.52, 10 mmol) and absolute ethanol (50 ml) were refluxed for 2 hours. On cooling, the salt separated and was recrystallized from absolute ethanol to give the title compound (1.59 g), m.p. 189–190° C. (dec).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07022719B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-702fba7bf9704f0a87e1d57d66805d25 |
| Source note | uspto-grants-2006_04 |