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HRID1794065

反应详情

EQUATION

反应方程式

HRID 1794065 的结构方程式

REACTANTS

反应物

2
结构：ClCc1ccc(Cl)cc1
HCID7723

4-Chlorobenzyl chloride

C7H6Cl2

结构：C[C@@H]1CNC[C@H](C)N1C(=O)OC(C)(C)C
HCID21021901

tert-Butyl (2R,6S)-2,6-dimethylpiperazine-1-carboxylate

C11H22N2O2

PRODUCTS

生成物

1
结构：C[C@@H]1CNC[C@H](C)N1C(=O)OCc1ccc(Cl)cc1.Cl
HCID69141647

未命名化合物

PROCEDURE

实验过程

Prepared in analogy to Example 25 with cis-N-Boc-2,6-dimethyl-piperazine and 4-chloro-benzyl chloride. Colourless powder, 1H-NMR (d6-DMSO): 1.30 d 7.2 Hz, 6H; 3.0–3.25 m, 4H and 4.2–4.4 m, 2H; 5.11 s, 2H; 7.35–7.55 AB-system, 4H; 9.5 br, 2H. MS (ISP): 283.1 (M+H)+.

WORKUP

后处理

  1. custom5.11 s, 2H