HRID1794134

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID22219889

(3-Bromo-2,6-difluorophenyl)methanol

C7H5BrF2O

结构：C[C@@H]1CN(C(=O)OC(C)(C)C)C[C@H](C)N1C(=O)Cl

HCID86585999

rel-1,1-Dimethylethyl (3R,5S)-4-(chlorocarbonyl)-3,5-dimethyl-1-piperazinecarboxylate

C12H21ClN2O3

PRODUCTS

生成物

结构：C[C@@H]1CN(C(=O)OC(C)(C)C)C[C@H](C)N1C(=O)OCc1c(F)ccc(Br)c1F

HCID69141723

未命名化合物

PROCEDURE

实验过程

The compound was prepared from (3-bromo-2,6-difluoro-phenyl)-methanol and 4-chlorocarbonyl-cis-3,5-dimethyl-piperazine-1-carboxylic acid tert-butyl ester according to the procedures described in Example 121 and 54 to give the product as a colorless oil (9.75 g); MS (ISP): 482.3 (M+NH4)+.