HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22219846, compound → HCID 86586003, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22219846 | HCID 22219846 | — |
| Reactant | (R)-4-Chlorocarbonyl-3-ethyl-piperazine-1-carboxylic acid tert-butyl ester | HCID 86586001 | — |
| Product | HCID 86586003 | HCID 86586003 | 80% |
Reaction Steps
This compound was prepared from 2-chloro-6-fluoro-4-prop-2-ynyloxy-benzylalcohol and (R)-4-chlorocarbonyl-3-ethyl-piperazine-1-carboxylic acid tert-butyl ester according to the procedure described in Example 179 to give the product as a colorless oil (357 mg; 80%); MS (ISP): 472.3 (M+NH4)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07022707B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-02a2f01c73964f79b05322ad53fc5a0a |
| Source note | uspto-grants-2006_04 |