Diethyl Ether → HCID 87929606, compound

HRID 1794176Notes

Reaction equation

Cl.[CH2:2]([O:4][C:5]1[CH:6]=[C:7]([C:14]2[C@@H:23]3[C@@H:18]([CH2:19][CH:20]=[CH:21][CH2:22]3)[C:17](=[O:24])[N:16]([C:25]3[CH:30]=[CH:29][C:28]([C:31]([N:33]4[CH2:38][CH2:37][N:36]([C:39]5C=CC=CC=5)[CH2:35][CH2:34]4)=[O:32])=[CH:27][CH:26]=3)[N:15]=2)[CH:8]=[CH:9][C:10]=1[O:11][CH2:12][CH3:13])[CH3:3].C([O:47]CC)C>>[CH2:2]([O:4][C:5]1[CH:6]=[C:7]([C:14]2[C@@H:23]3[C@@H:18]([CH2:19][CH:20]=[CH:21][CH2:22]3)[C:17](=[O:24])[N:16]([C:25]3[CH:26]=[CH:27][C:28]([C:31]([N:33]4[CH2:38][CH2:37][N:36]([CH:39]=[O:47])[CH2:35][CH2:34]4)=[O:32])=[CH:29][CH:30]=3)[N:15]=2)[CH:8]=[CH:9][C:10]=1[O:11][CH2:12][CH3:13])[CH3:3]

Participants

Reactant 2

HCID 3283Diethyl Ether

HCID 69641867HCID 69641867, compound

Product 1

HCID 87929606HCID 87929606, compound

Procedure

Prepared from intermediate product A1 and piperazinylcarbaldehyde as described for compound 1. Cystallised from diethyl ether as the free base. M.p. 143–144° C.

Sources & evidence

ORD record: ord-100b62f1614e4b4db3653a134b8e7f48
Source dataset: uspto-grants-2006_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07022696B2

Reaction notes

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