1-[3-(Dimethylamino)propyl]piperazine → HCID 69642129, compound

HRID 1794180Notes

Reaction equation

HRID 1794180 reaction equation
[CH3:1][N:2]([CH3:12])[CH2:3][CH2:4][CH2:5][N:6]1[CH2:11][CH2:10][NH:9][CH2:8][CH2:7]1.[ClH:13].[CH3:14][O:15][C:16]1[C:24]2[O:23][C:22](C)(C)C[C:20]=2[C:19]([C:27]2[C@@H:36]3[C@@H:31]([CH2:32][CH:33]=[CH:34][CH2:35]3)[C:30](=[O:37])[N:29]([C:38]3[CH:43]=[CH:42][C:41]([C:44](N4CCN(C/C=C/C5C=CC=CC=5)CC4)=[O:45])=[CH:40][CH:39]=3)[N:28]=2)=[CH:18][CH:17]=1>>[ClH:13].[ClH:13].[CH3:22][O:23][C:24]1[CH:20]=[C:19]([C:27]2[C@@H:36]3[C@@H:31]([CH2:32][CH:33]=[CH:34][CH2:35]3)[C:30](=[O:37])[N:29]([C:38]3[CH:39]=[CH:40][C:41]([C:44]([N:9]4[CH2:8][CH2:7][N:6]([CH2:5][CH2:4][CH2:3][N:2]([CH3:1])[CH3:12])[CH2:11][CH2:10]4)=[O:45])=[CH:42][CH:43]=3)[N:28]=2)[CH:18]=[CH:17][C:16]=1[O:15][CH3:14]

Participants

3

Reactant 2

HCID 27362341-[3-(Dimethylamino)propyl]piperazineHCID 69642098HCID 69642098, compound

Product 1

HCID 69642129HCID 69642129, compound

Procedure

Prepared from intermediate product A6 and 1-(3-dimethylaminopropyl)piperazine as described for compound 8. M.p. 223–226° C.

Sources & evidence

ORD record
ord-a09e8fd392b94a8791d38b904adf50bf
Source dataset
uspto-grants-2006_04
Patent number
US07022696B2

Reaction notes

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