4-Chloroindole → HCID 10201662, compound

HRID 1794195Notes

Reaction equation

HRID 1794195 reaction equation
[Cl:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]2[C:3]=1[CH:4]=[CH:5][NH:6]2.O[CH2:12][C:13]1[O:19][C:16]([CH:17]=[O:18])=[CH:15][CH:14]=1>>[Cl:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]2[C:3]=1[C:4]([CH:12]([C:4]1[C:3]3[C:7](=[CH:8][CH:9]=[CH:10][C:2]=3[Cl:1])[NH:6][CH:5]=1)[C:13]1[O:19][C:16]([CH2:17][OH:18])=[CH:15][CH:14]=1)=[CH:5][NH:6]2

Participants

3

Reactant 2

HCID 913454-ChloroindoleHCID 2373325-(Hydroxymethyl)furfural

Product 1

HCID 10201662HCID 10201662, compound

Procedure

The compound Bis(4-chloroindol-3-yl)-(5-hydroxymethylfuran-2-yl)methane was prepared following procedure A, starting from 4-chloro indole and 5-hydroxymethyl furfural. LC: Tr 2.84 min, MS: 411 (M+H)+

Workup

  1. customTr 2.84 min, MS

Sources & evidence

ORD record
ord-5b382b387f3a4e29a7023e97fd41bd5c
Source dataset
uspto-grants-2006_04
Patent number
US07022730B2

Reaction notes

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