2,4-Difluorobenzaldehyde → HCID 10137327, compound

HRID 1794197Notes

Reaction equation

HRID 1794197 reaction equation
[Cl:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]2[C:3]=1[CH:4]=[CH:5][NH:6]2.[F:11][C:12]1[CH:19]=[C:18]([F:20])[CH:17]=[CH:16][C:13]=1[CH:14]=O>>[Cl:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]2[C:3]=1[C:4]([CH:14]([C:4]1[C:3]3[C:7](=[CH:8][CH:9]=[CH:10][C:2]=3[Cl:1])[NH:6][CH:5]=1)[C:13]1[CH:16]=[CH:17][C:18]([F:20])=[CH:19][C:12]=1[F:11])=[CH:5][NH:6]2

Participants

3

Reactant 2

HCID 737702,4-DifluorobenzaldehydeHCID 913454-Chloroindole

Product 1

HCID 10137327HCID 10137327, compound

Procedure

The compound Bis(4-chloroindol-3-yl)-(2,4-difluorophenyl)methane was prepared following procedure A, starting from 4-chloro indole and 2,4-difluoro benzaldehyde. LC: Tr 2.63 min, MS: 427 (M+H)+

Workup

  1. customTr 2.63 min, MS

Sources & evidence

ORD record
ord-6b00d6aadf6c41dd8af863fdaa2a85aa
Source dataset
uspto-grants-2006_04
Patent number
US07022730B2

Reaction notes

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