6-Chloroindole → HCID 10138354, compound

HRID 1794198Notes

Reaction equation

HRID 1794198 reaction equation
[Cl:1][C:2]1[CH:10]=[C:9]2[C:5]([CH:6]=[CH:7][NH:8]2)=[CH:4][CH:3]=1.[Cl:11][C:12]1[CH:19]=[C:18]([F:20])[CH:17]=[CH:16][C:13]=1[CH:14]=O>>[Cl:1][C:2]1[CH:10]=[C:9]2[C:5]([C:6]([CH:14]([C:6]3[C:5]4[C:9](=[CH:10][C:2]([Cl:1])=[CH:3][CH:4]=4)[NH:8][CH:7]=3)[C:13]3[CH:16]=[CH:17][C:18]([F:20])=[CH:19][C:12]=3[Cl:11])=[CH:7][NH:8]2)=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 871116-ChloroindoleHCID 1450242-Chloro-4-fluorobenzaldehyde

Product 1

HCID 10138354HCID 10138354, compound

Procedure

The compound Bis(6-chloroindol-3-yl)-(4-fluoro-2-chlorophenyl)methane was prepared following procedure A, starting from 6-chloro indole and 2-chloro 4-fluoro benzaldehyde. LC: Tr 2.79 min, MS: 443 (M+H)+

Workup

  1. customTr 2.79 min, MS

Sources & evidence

ORD record
ord-89952c3953b94e739b1ad97757a55a4d
Source dataset
uspto-grants-2006_04
Patent number
US07022730B2

Reaction notes

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