1-Methylindole → HCID 9947562, compound

HRID 1794200Notes

Reaction equation

HRID 1794200 reaction equation
[CH3:1][N:2]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3]1.O[CH2:12][C:13]1[O:19][C:16]([CH:17]=[O:18])=[CH:15][CH:14]=1>>[CH3:1][N:2]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[C:4]([CH:12]([C:4]2[C:5]3[C:10](=[CH:9][CH:8]=[CH:7][CH:6]=3)[N:2]([CH3:1])[CH:3]=2)[C:13]2[O:19][C:16]([CH2:17][OH:18])=[CH:15][CH:14]=2)=[CH:3]1

Participants

3

Reactant 2

HCID 117811-MethylindoleHCID 2373325-(Hydroxymethyl)furfural

Product 1

HCID 9947562HCID 9947562, compound

Procedure

The compound Bis(1-methylindol-3-yl)-(5-hydroxymethyl-2-furyl)methane was prepared following general procedure A, starting from N-methyl indole and 5-hydroxy methyl furfural. LC: Tr 2.25 min, MS: 371 (M+H)+

Workup

  1. customTr 2.25 min, MS

Sources & evidence

ORD record
ord-2dd56a59d4e745f7b6d59d3ea10f8ac8
Source dataset
uspto-grants-2006_04
Patent number
US07022730B2

Reaction notes

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