5-(Hydroxymethyl)furfural → HCID 10160375, compound

HRID 1794201Notes

Reaction equation

HRID 1794201 reaction equation
[CH3:1][N:2]1[C:10]2[C:5](=[C:6]([Cl:11])[CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3]1.O[CH2:13][C:14]1[O:20][C:17]([CH:18]=[O:19])=[CH:16][CH:15]=1>>[Cl:11][C:6]1[CH:7]=[CH:8][CH:9]=[C:10]2[C:5]=1[C:4]([CH:13]([C:4]1[C:5]3[C:10](=[CH:9][CH:8]=[CH:7][C:6]=3[Cl:11])[N:2]([CH3:1])[CH:3]=1)[C:14]1[O:20][C:17]([CH2:18][OH:19])=[CH:16][CH:15]=1)=[CH:3][N:2]2[CH3:1]

Participants

3

Reactant 2

HCID 2373325-(Hydroxymethyl)furfuralHCID 130487594-Chloro-1-methyl-1H-indole

Product 1

HCID 10160375HCID 10160375, compound

Procedure

The compound Bis(4-chloro-1-methylindol-3-yl)-(5-hydroxymethyl-2-furyl)methane was prepared following procedure A, starting from N-methyl 4-chloro indole and 5-hydroxy methyl furfural. LC: Tr 2.73 min, MS: 439 (M+H)+

Workup

  1. customTr 2.73 min, MS

Sources & evidence

ORD record
ord-cbbce96b5e1d44a3a3122b8c964d27da
Source dataset
uspto-grants-2006_04
Patent number
US07022730B2

Reaction notes

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