5-chloro-3-phenyl-4-Isoxazolecarboxaldehyde → HCID 22220922, compound

Participants

Reaction Steps

5-Chloro-3-phenylisoxazole 4-carboxaldehyde (1.1 g) and (6-bromo-3H-isoindol-1-yl)hydrazine (1.2 g, 5.3 mmol) were reacted in a similar manner to that described in Example 4 to give the title compound (415 mg, 19%). 1H NMR (400 MHz, d6-DMSO) δ 8.161–8.165 (1H, m), 7.71–7.74 (1H, m), 7.47–7.61 (6H, m), 4.83 (2H, s).

Provenance & Evidence