HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1794521Generated: October 29, 2026
Pyridinium chloride → HCID 10149371, compound
https://huagongshe.com/reaction/1794521
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | HCID 22221599 | HCID 22221599 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 10149371 | HCID 10149371 | — |
Reaction Steps
Compound 88 was treated with Pyridine HCl (5 g) and heated to 200° C. After 1 hr, the reaction was cooled and diluted with water. The aqueous layer was extracted with EtOAc, dried over MgSO4, and the product was purified by column chromatography (eluant 25% EtOAc/hexanes) to give the product as a solid: (0.025 g, 4.8%); MS 277 [M−H]−
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07022733B2 |
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| Source dataset | uspto-grants-2006_04 |
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| ORD ID | ord-79ff1f5483c5410ea50681e35688b8b6 |
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| Source note | uspto-grants-2006_04 |
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