4-Pentenal → HCID 69463025, compound
Reaction equation
[C:1]([N:5]1[C:9]2[CH:10]=[CH:11][CH:12]=[CH:13][C:8]=2[O:7][C:6]1=[O:14])(=[O:4])[CH2:2][CH3:3].[CH:15](=[O:20])[CH2:16][CH2:17][CH:18]=[CH2:19]>>[CH3:3][C@H:2]([C@@H:15]([OH:20])[CH2:16][CH2:17][CH:18]=[CH2:19])[C:1]([N:5]1[C:9]2[CH:10]=[CH:11][CH:12]=[CH:13][C:8]=2[O:7][C:6]1=[O:14])=[O:4]Participants
3
Procedure
Was prepared according to the method of paragraph C by reaction of N-propionyl-2-benzoxazolinone with 4-pentenal. 13C-NMR (CDCl3, 100 MHz): δ 176.28, 151.07, 142.20, 137.96, 127.75, 125.50, 124.89, 116.26, 115.19, 109.89, 70.93, 43.76, 33.12, 30.16, 10.21.
Workup
- customWas prepared
Sources & evidence
- ORD record
- ord-0a374dfa39bb4e84a221fc3e808f3ca2
- Source dataset
- uspto-grants-2006_04
- Patent number
- US07022825B2
Reaction notes
Loading…