3-Propionyl-2-benzoxazolinone → HCID 69463427, compound

HRID 1794572Notes

Reaction equation

HRID 1794572 reaction equation
[C:1]([N:5]1[C:9]2[CH:10]=[CH:11][CH:12]=[CH:13][C:8]=2[O:7][C:6]1=[O:14])(=[O:4])[CH2:2][CH3:3].[CH3:15][O:16][CH2:17][CH2:18][O:19][CH2:20][CH:21]=[O:22]>>[CH3:15][O:16][CH2:17][CH2:18][O:19][CH2:20][C@@H:21]([OH:22])[C@@H:2]([CH3:3])[C:1]([N:5]1[C:9]2[CH:10]=[CH:11][CH:12]=[CH:13][C:8]=2[O:7][C:6]1=[O:14])=[O:4]

Participants

3

Reactant 2

HCID 8437913-Propionyl-2-benzoxazolinoneHCID 14251035(2-Methoxyethoxy)acetaldehyde

Product 1

HCID 69463427HCID 69463427, compound

Procedure

Prepared according to the method of paragraph C by reaction of N-propionyl-2-benzoxazolinone with (2-methoxyethoxy)acetaldehyde. 13C-NMR (CDCl3, 100 MHz): δ 175.01, 151.02, 142.18, 127.91, 125.30, 124.77, 116.15, 109.76, 73.23, 71.86, 70.73, 70.64, 58.88, 41.63, 11.88.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-3a7c7a2b80014f5490558009f072da68
Source dataset
uspto-grants-2006_04
Patent number
US07022825B2

Reaction notes

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