反应详情

The title compound was prepared from (R)-2-methyl-CBS-oxazaborolidine monohydrate and 3-(2-bromoacetyl)pyridine hydrobromide in substantially the same manner, as described in Example 123. The product was obtained as an oil; 1H NMR (300 MHz, DMSO-d6) δ 2.94–2.97 (m, 1 H), 3.14–3.17 (m, 1 H), 3.99–4.01 (m, 1 H), 7.36–7.40 (m, 1 H), 7.63–7.66 (m, 1 H), 8.51–8.55 (m, 2 H); MS (ES) m/z: 121 (M+).

1. customThe product was obtained as an oil