HCID 22184374, compound → HCID 22184375, compound

HRID 1794980Notes

Reaction equation

HRID 1794980 reaction equation
[CH3:1][O:2][CH2:3][C:4]1[CH2:8][CH2:7][C:6](=[O:9])[C:5]=1[CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]>[Pd]>[CH3:1][O:2][CH2:3][CH:4]1[CH2:8][CH2:7][C:6](=[O:9])[CH:5]1[CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]

Participants

3

Reactant 1

HCID 22184374HCID 22184374, compound

Product 1

HCID 22184375HCID 22184375, compound

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

Using a standard autoclave pressure reactor 3-(methoxymethyl)-2-pentylcyclopent-2-en-1-one (0.5 mol) was hydrogenated at 100° C. and 200 pounds per square inch using 5% palladium on carbon as a catalyst. After filtration, 3-(methoxymethyl)-2-pentylcyclopentan-1-one was obtained as was confirmed by the following data;

Workup

  1. customwas hydrogenated at 100° C.
  2. filtrationAfter filtration

Sources & evidence

ORD record
ord-391238dff3104043a816ac6b8b1045af
Source dataset
uspto-grants-2006_04
Patent number
US07026279B2

Reaction notes

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