HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenacyl bromide → HCID 22185807, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenacyl bromide | HCID 6259 | — |
| Reactant | 4-(aminosulfonyl)benzeneacetic acid | HCID 6483854 | — |
| Reactant | HCID 22185801 | HCID 22185801 | — |
| Product | HCID 22185807 | HCID 22185807 | 40% |
Reaction Steps
The title compound was synthesized in a manner similar to that described for 47b from 4-sulfamoylphenylacetic acid and 2-bromoacetophenone in 40% yield. 1H NMR (DMSO-d6) δ 5.43 (s, 2H), 7.36–7.45 (m, 5), 7.76 (d, J=8.5 Hz, 2H), 7.96 (d, J=8.5 Hz, 2H); HRMS calc'd for M+ 315.0557. found 315.0573. Anal. (C16H13NO4S) C, H, N.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07026346B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-43a3d898d5b64c729b6bca467f4c8ffa |
| Source note | uspto-grants-2006_04 |