HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2-(1h-Pyrazol-3-yl)-benzylamine hydrochloride salt
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178453037 | HCID 178453037 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2-(1h-Pyrazol-3-yl)-benzylamine hydrochloride salt | HCID 178479178 | — |
Reaction Steps
hydrogen chloride gas was bubbled through a 0° C. solution of tert-butyl 2-(1H-pyrazol-3-yl)benzylcarbamate (60 mg, 0.220 mmol) in ethyl acetate (5 ml) for 2 min and stirred for 40 min. A precipitate formed, and the suspension was concentrated in vacuo to give 2-(1H-pyrazol-3-yl)-benzylamine hydrochloride salt; MS (ES+) M+1 174.1 for C10H11N3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07026324B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-4b9e7267a4a74d259bccad4c8bb88b5c |
| Source note | uspto-grants-2006_04 |