HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → N-Methyl-2-(naphthalen-2-yl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Ethyl 2-naphthylacetate | HCID 256821 | — |
| Product | N-Methyl-2-(naphthalen-2-yl)acetamide | HCID 13501064 | — |
Reaction Steps
A mixture of naphthalen-2-yl-acetic acid ethyl ester (42.8 g, 200 mmol) and 64 mL of methylamine (40 wt % in H2O) were stirred at room temperature overnight. Then the white precipitate was filtered off and washed with water. After drying in vacuum the title compound was obtained as a white solid. MS (ES+): 226 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07026326B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-34a9a8e5aed2438f8ffd075b5dd84221 |
| Source note | uspto-grants-2006_04 |