HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(6-Bromohexyl)benzene → 2-Acetamido-1,3-bis(tert-butyldimethylsilyloxy)-2-(2-(4-(1-hydroxy-7-phenylheptyl)phenyl)ethyl)propane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (6-Bromohexyl)benzene | HCID 561788 | — |
| Edukt | 2-Acetamido-1,3-bis(tert-butyldimethylsilyloxy)-2-(2-(4-formylphenyl)ethyl)propane | HCID 15516678 | — |
| Produkt | 2-Acetamido-1,3-bis(tert-butyldimethylsilyloxy)-2-(2-(4-(1-hydroxy-7-phenylheptyl)phenyl)ethyl)propane | HCID 22178488 | 65,2% |
Reaktionsschritte
2-Acetamido-1,3-bis(tert-butyldimethylsilyloxy)-2-(2-(4-formylphenyl)ethyl)propane (3.0 g) and 1-bromo-6-phenylhexane (3.1 g) were reacted and treated in the same manner as in Working example 1(6) to give the title compound (2.6 g) as a pale yellow oily substance.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | USRE039072E1 |
| Quelldatensatz | uspto-grants-2006_04 |
| ORD ID | ord-74127cf9fc164ce7bdd3037ae9ac727f |
| Quellennotiz | uspto-grants-2006_04 |