HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 22179844, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 22179838 | HCID 22179838 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22179844 | HCID 22179844 | — |
Reaction Steps
A solution of Example 5B (671 mg, 1.725 mmol) in dichloromethane (2 mL) at room temperature was treated with TFA (1.8 mL) and water (0.2 mL) allowed to stand for 2 hours The solution was concentrated to provide the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07030115B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-755bbdc9832b47fe83485cf709de13ad |
| Source note | uspto-grants-2006_04 |