HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium hydride → 4-(3,6-Dimethoxyphenylsulphanyl)-2-amino-nitrobenzene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium hydride | HCID 24758 | — |
| Edukt | 2,5-Dimethoxythiophenol | HCID 519009 | — |
| Edukt | 4-(4-Hydroxyphenylsulphanyl)-2-amino-nitrobenzene | HCID 22180683 | — |
| Produkt | 4-(3,6-Dimethoxyphenylsulphanyl)-2-amino-nitrobenzene | HCID 22180700 | — |
Reaktionsschritte
Using the general method described for 4-(4-hydroxyphenylsulphanyl)-2-amino-nitrobenzene in Example 2, except that one equivalent of NaH was used, 4-(3,6-dimethoxyphenylsulphanyl)-2-amino-nitrobenzene (4.19 g) was prepared from 3,6-dimethoxybenzenethiol (2.55 g; 15 mmol).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07030123B2 |
| Quelldatensatz | uspto-grants-2006_04 |
| ORD ID | ord-5c4db8bb278e4e6fa09fc86a1ca03b64 |
| Quellennotiz | uspto-grants-2006_04 |