HRID1795931

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID36904

2,3,4-Trichlorobenzenesulfonyl chloride

C6H2Cl4O2S

HCID587874

2-Amino-5,5-dimethyl-5,6-dihydro-4H-benzothiazol-7-one

C9H12N2OS

PRODUCTS

产物

反应SMILES：CC1(C)CC(=O)c2sc(NS(=O)(=O)c3ccc(Cl)c(Cl)c3Cl)nc2C1

HCID10296979

2,3,4-Trichloro-N-(4,5,6,7-tetrahydro-5,5-dimethyl-7-oxo-2-benzothiazolyl)benzenesulfonamide

C15H13Cl3N2O3S2

PROCEDURE

实验过程

The title compound was prepared from 2-amino-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)-one (53 mg) and 2,3,4-trichlorobenzenesulfonyl chloride (76 mg) as described in the synthetic METHOD B to give a white solid (47.2 mg) with purity >90%: MS (pos) m/z 439.3, 441.3; HRMS m/z 437.9451 (calc. of monoisotopic mass for C15H13Cl3N2O3S2 gives 437.9433).