HRID1795932

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID587874

2-Amino-5,5-dimethyl-5,6-dihydro-4H-benzothiazol-7-one

C9H12N2OS

HCID2797220

4-bromo-5-chlorothiophene-2-sulfonyl chloride

C4HBrCl2O2S2

PRODUCTS

生成物

结构：CC1(C)CC(=O)c2sc(NS(=O)(=O)c3cc(Br)c(Cl)s3)nc2C1

HCID10276050

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 2-amino-5,5-dimethyl-5,6-dihydro-1,3-benzothiazol-7(4H)one (53 mg) and 4-bromo-5-chlorothiophene-2-sulfonyl chloride (80 mg) as described in the synthetic METHOD B to give a white-yellow solid (47.1 mg) with purity >90%: MS (pos) m/z 455.2, 457.2.