HCID 3822419, compound → HCID 22181471, compound
Reaction equation
[NH:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[CH2:10]N1C2C=CC=CC=2N=N1.[CH3:20][C:21]1[C:29]([CH3:30])=[CH:28][C:24]2[NH:25][N:26]=[N:27][C:23]=2[CH:22]=1>>[NH:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[CH2:10][N:27]1[C:23]2[CH:22]=[C:21]([CH3:20])[C:29]([CH3:30])=[CH:28][C:24]=2[N:25]=[N:26]1Participants
3
Procedure
The same procedure described in the preparation of 1-(1H-benzimidazol-2-ylmethyl)-1H-benzotriazole was used, except that 5,6-dimethylbenzotriazole was used instead of benzotriazole. 1-(1H-benzimidazol-2-ylmethyl)-5,6-dimethyl-1H-benzotriazole was isolated as an intermediate:
Sources & evidence
- ORD record
- ord-4d83457759734542b0027290bb280a25
- Source dataset
- uspto-grants-2006_04
- Patent number
- US07030140B2
Reaction notes
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