Glycidyl methacrylate → HCID 22182321, compound

HRID 1796572Notes

Reaction equation

HRID 1796572 reaction equation
[C:1]([O:6][CH2:7][CH:8]1[O:10][CH2:9]1)(=[O:5])[C:2]([CH3:4])=[CH2:3].[C:11]1(=[O:17])[NH:15][C:14](=[O:16])[CH2:13][CH2:12]1.[Cl-].C(CCN(CC)CC)C1C=CC=CC=1.C1(=O)CCCCC1>>[C:14]1(=[O:16])[NH:15][C:11](=[O:17])[CH2:12][CH2:13]1.[C:1]([O:6][CH2:7][CH:8]1[O:10][CH2:9]1)(=[O:5])[C:2]([CH3:4])=[CH2:3]

Participants

5

Reactant 4

HCID 7837Glycidyl methacrylateHCID 7967CyclohexanoneHCID 11439SuccinimideHCID 24185694HCID 24185694, compound

Product 1

HCID 22182321HCID 22182321, compound

Procedure

22.7 g (0.16 mol) of glycidyl methacrylate, 15.5 g (0.16 mol) of succinimide and 1.0 g (4.0 mmol) of benzyltriethylamine chloride were placed into a suitably sized reaction vessel fitted with a stirrer and a nitrogen gas source. 200 g of cyclohexanone were added to dissolve the materials. The mixture was stirred at a temperature of about 105 to about 120° C. for 24 hours until the reaction was completed. The reaction yielded 238 g in total amount of solution, which contained 16 wt % of the succinimide-GMA adduct.

Workup

  1. customfitted with a stirrer
  2. dissolutionto dissolve the materials
  3. customThe reaction yielded 238 g in total amount of solution, which

Sources & evidence

ORD record
ord-829b4792713e47b490a909e194fd7235
Source dataset
uspto-grants-2006_04
Patent number
US07030201B2

Reaction notes

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