HuagongsheHuagongshe Chemistry Print Report · For research reference only
Picolyl chloride hydrochloride → 7-nitro-2-(pyridin-2-yl)methyl-2H-phthalazin-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Picolyl chloride hydrochloride | HCID 23392 | — |
| Reactant | 7-Nitrophthalazin-1(2h)-one | HCID 277729 | — |
| Product | 7-nitro-2-(pyridin-2-yl)methyl-2H-phthalazin-1-one | HCID 22180252 | — |
Reaction Steps
Step (b) of Example 125 was repeated, except that the compound prepared in step (b) of Example 137 and 2-(chloromethyl)pyridine hydrochloride were used as the starting compounds. Thus, 7-nitro-2-(pyridin-2-yl)methyl-2H-phthalazin-1-one was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07030120B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-612e6398bac4439ca472e51fd9f2ebf2 |
| Source note | uspto-grants-2006_04 |