Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetyl chloride → 4-(2,3-Dimethoxy-benzylidene)-morpholin-4-ium chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetyl chloride | HCID 6367 | — |
| 반응물 | Morpholine | HCID 8083 | — |
| 반응물 | 2,3-Dimethoxybenzaldehyde | HCID 66581 | — |
| 생성물 | 4-(2,3-Dimethoxy-benzylidene)-morpholin-4-ium chloride | HCID 22174759 | — |
반응 단계
The reaction of 7.3 ml (0.084 mol) morpholine and 5.8 g (0.035 mol) 2,3-dimethoxybenzaldehyde in accordance with general synthesis instructions 2 and subsequent reaction with 2.1 ml (0.035 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 5.6 g (corresponding to 59% of the yield calculated by theory) 4-(2,3-dimethoxy-benzylidene)-morpholin-4-ium chloride
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07034018B2 |
| 출처 데이터셋 | uspto-grants-2006_04 |
| ORD ID | ord-f4d9ff6b2d1043ae94f3f4eb2dd82422 |
| 출처 메모 | uspto-grants-2006_04 |