HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 69617874, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 22177214 | HCID 22177214 | — |
| Catalyst | Sulfuric Acid | HCID 1118 | — |
| Product | HCID 69617874 | HCID 69617874 | — |
Reaction Steps
A solution of 2-(3-nitrophenyl)furan-3-carboxylic acid (1.2 g) in methanol (200 mL) containing concentrated sulfuric acid (5 drops) was heated under reflux for 18 h. The reaction solution was evaporated to dryness under reduced pressure to give the title compound as a yellow solid (0.66 g). m.p.=93–94° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07034053B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-c3ca52953dba4feeb685aacafecc5dea |
| Source note | uspto-grants-2006_04 |