Water → HCID 9899843, compound

Participants

Reaction Steps

Acetic acid anhydride (1.2 mL) was added to a solution of 1-(2-bromophenyl)-2-propanol (529 mg) in pyridine (1.0 mL) at 20° C. under stirring. The reaction mixture was stirred overnight, then poured into a mixture of water and EtOAc. The aqueous phase was extracted with more EtOAc (×2). The combined organic phases were washed with water (×3), dried (MgSO4), filtered and concentrated in vacuo to afford the title compound as a syrup.

Provenance & Evidence