Sodium Iodide → HCID 22174498, compound

Participants

Reaction Steps

Compound 164 (1.72 g, 2.73 mmol) was dissolved in dry acetone (2.7 mL) and dry NaI (0.82 g, 5.47 mmol) was added. The suspension was stirred in a light protected flask at room temperature for 20 h after which the reaction mixture was diluted with water and the water phase was extracted three times with EtOAc. The combined organic phases were washed with brine, dried (MgSO4), filtered and evaporated in vacuo. This afforded the title compound as a yellow oil.

Provenance & Evidence