HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylcarbodiimide → 6-chlorohexyl (2E)-3-(4-butoxy-3-methoxyphenyl)-2-propenoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | 6-Chloro-1-hexanol | HCID 74828 | — |
| Reactant | 3-(4-Butoxy-3-methoxyphenyl)prop-2-enoic acid | HCID 5933564 | — |
| Reactant | 4-(Dimethylamino)pyridinium 4-toluenesulfonate | HCID 11185494 | — |
| Product | 6-chlorohexyl (2E)-3-(4-butoxy-3-methoxyphenyl)-2-propenoate | HCID 86594318 | — |
Reaction Steps
Preparation was carried out analogously to Example 5 using 4.24 g (16.94 mmol) (2E)-3-(4-butoxy-3-methoxyphenyl)-2-propenoic acid, 2.20 g (16.13 mmol) 6-chloro-1-hexanol, 1.90 g (6.45 mmol) 4-(dimethylamino)pyridinium p-toluenesulfonate and 4.16 g (20.17 mmol) N,N′-dicyclohexylcarbodiimide to give 6-chlorohexyl (2E)-3-(4-butoxy-3-methoxyphenyl)-2-propenoate as colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07034098B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-4607200730c641c88a1767a34e4b86e7 |
| Source note | uspto-grants-2006_04 |