HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylhydrazine → HCID 178515218, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylhydrazine | HCID 7516 | — |
| Reactant | Ethyl 4-chloro-6,7-difluoroquinoline-3-carboxylate | HCID 1511944 | — |
| Reactant | HCID 178515184 | HCID 178515184 | — |
| Product | HCID 178515218 | HCID 178515218 | — |
Reaction Steps
The title compound was prepared following the procedure described in Step 3 for the synthesis of 4a, using 3c and phenyl hydrazine. 1H NMR (DMSO-d6) δ (ppm):7.18 (1H, t, J=7.82 Hz), 7.43 (2H, dd, J=8.30, 7.33 Hz), 7.75 (1H, dd, J=11.22, 7.32 Hz), 8.18, 3H, m), 8.90 (1H, s). m/z 298.2 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08343957B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-4e81e0f01baa453b9ebe7b3a4f91c0b3 |
| Source note | uspto-grants-2013_01 |