HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylhydrazine → HCID 178488062, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylhydrazine | HCID 7516 | — |
| Reactant | Ethyl 4-chloro-6-methoxyquinoline-3-carboxylate | HCID 304558 | — |
| Product | HCID 178488062 | HCID 178488062 | — |
Reaction Steps
The title compound was prepared following the procedure described in Step 3 using 3d and phenyl hydrazine. 1H NMR (DMSO-d6) δ (ppm): 3.90 (3H, s), 7.17 (1H, m), 7.27 (1H, dd, J=9.06, 2.64 Hz), 7.40 (2H, m), 7.57 (1H, d, J=3.02 Hz), 7.67 (1H, d, J=9.06 Hz), 8.20 (2H, m), 8.63 (1H, s). m/z 292.3 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08343957B2 |
| Source dataset | uspto-grants-2013_01 |
| ORD ID | ord-f37a2ab5f14d4dc4b28d424d59bba49d |
| Source note | uspto-grants-2013_01 |